3-(2-呋喃基)丙酸乙酯合成路线 （共 24 条）
反应条件
hydrogen; Wilkinson's catalist in tetrahydrofuran T=45°C; P=2585.81 Torr; 18 h;
参考文献
Warner-Lambert Company
Patent: US6710190 B1, 2004 ;
Location in patent: Page column 30 ;
反应条件
nickel monoaluminide in ethyl acetate
参考文献
US4388317 A1, ;
US 4388317 A
反应条件
1: oxalyl chloride; dimethylformamide / CH2Cl2 / 3.5 h / 0 °C 2: 1.05 g / triethylamine View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 31 p. 5194 - 5197
反应条件
1: pyridine, piperidine 2: 100 percent / tri-n-propylamine / acetone / 2 h / Heating 3: 80 percent / conc. NH4OH, H2 / Raney nickel / ethanol View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 24, p. 65 - 72
反应条件
1: 100 percent / tri-n-propylamine / acetone / 2 h / Heating 2: 80 percent / conc. NH4OH, H2 / Raney nickel / ethanol View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 24, p. 65 - 72
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene Heating;
参考文献
Ishibashi; Mino; Sakata; Inada; Ikeda
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 5 p. 1148 - 1151
参考文献
Kaiser, Stefan; Smidt, Sebastian P.; Pfaltz, Andreas
Angewandte Chemie - International Edition, 2006 , vol. 45, # 31 p. 5194 - 5197
反应条件
toluene-4-sulfonic acid T=79°C; 60 h;
参考文献
Gazzetta Chimica Italiana, , vol. 111, # 11/12 p. 511 - 514
反应条件
1: t-BuONa / tetrahydrofuran 2: H2 View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 47 p. 8345 - 8349
反应条件
1: sulfuryl chloride / CH2Cl2 / 1 h / 0 °C 2: 86 percent / TiCl4 / CH2Cl2 / -20 °C 3: 32 percent / Bu3SnH, azoisobutyronitrile / benzene / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 5 p. 1148 - 1151
