反应条件
in hexane Ar-atmosphere; stirring (25°C, 10 h); distillation off of hexane and HN(SiMe3)2 (vac.), addn. of hexanes, filtration, sublimation off of t-Bu3SiOSiMe3 (40°C, 1E-4 torr), recrystn. (hexanes, -78°C); elem. anal.;
参考文献
Inorganic Chemistry, , vol. 30, p. 2494 - 2508
