1,4-亚苯基二硼酸, 频哪醇二酯合成路线 （共 36 条）
反应条件
magnesium sulfate in methanol T=30°C;
参考文献
Chaumeil, Helene; Le Drian, Claude; Defoin, Albert
Synthesis, 2002 , # 6 p. 757 - 760
反应条件
1: p-bromophenyl bromide With n-butyllithium in tetrahydrofuran T=-78°C; 2 h; Inert atmosphere; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Zhou, Mingjie; Huang, Jie; Liu, Yijin
Patent: US2013/165646 A1, 2013 ;
Location in patent: Paragraph 0066; 0067; 0068 ;
反应条件
copper(l) iodide; tributyl-amine; potassium tert-butylate in tetrahydrofuran T=20°C;
参考文献
Kleeberg, Christian; Dang, Li; Lin, Zhenyang; Marder, Todd B.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5350 - 5354
Angewandte Chemie, 2009 , vol. 121, p. 5454 - 5458
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Ma, Yudao; Song, Chun; Jiang, Wei; Xue, Guoping; Cannon, John F.; Wang, Xiaomei; Andrus, Merritt B.
Organic Letters, 2003 , vol. 5, # 24 p. 4635 - 4638
反应条件
1: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 18 h; 2: 4-bromo-1-iodobenzene; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in 1,4-dioxane T=80°C; 18 h;
参考文献
US6680401 B1, ;
Page column 57 ;
反应条件
iodine; magnesium in tetrahydrofuran T=25°C; Barbier-type conditions; Inert atmosphere;
参考文献
Clary, Jacob W.; Rettenmaier, Terry J.; Snelling, Rachel; Bryks, Whitney; Banwell, Jesse; Wipke, W. Todd; Singaram, Bakthan
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9602 - 9610
反应条件
copper(l) iodide; tributyl-amine; potassium tert-butylate in tetrahydrofuran T=20°C;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 5350 - 5354
Angewandte Chemie, , vol. 121, p. 5454 - 5458
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane T=100°C; 24 h; Inert atmosphere;
参考文献
Britze, Antje; Jacob, Josemon; Choudhary, Veena; Moellmann, Vera; Grundmeier, Guido; Luftmann, Heinrich; Kuckling, Dirk
Polymer, 2010 , vol. 51, # 23 p. 5294 - 5303
反应条件
[2,2']bipyridinyl; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in neat (no solvent) at 80°C for 16 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 3 p. 390 - 391
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran byproducts: KI, C6H5Bpin; react. of (B(OC(CH3)2)2)2 (3 equiv.), 1,4-I2C6H4 (1 equiv.), CuI (10 molpercent), nBu3P (13 molpercent) and KOtBu (1.5 equiv.) at room temp.;
参考文献
Kleeberg, Christian; Dang, Li; Lin, Zhenyang; Marder, Todd B.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5350 - 5354
Angewandte Chemie, 2009 , vol. 121, p. 5454 - 5458
