3-(2-氯苯磺酰基)-丙酸合成路线 （共 6 条）
反应条件
1: With potassium hydroxide; ethanol; water
T=20°C; 64 h;
2: With hydrogenchloride; water
pH=1;
参考文献
EMISPHERE TECHNOLOGIES, INC.; WANG, Nai, Fang; SARAF, Sushma; PUSZTAY, Stephen, V.
Patent: WO2008/14430 A1, 2008 ;
Location in patent: Page/Page column 52 ;
反应条件
sodium hydroxide
Microwave irradiation;
参考文献
Ma, Zhengyue; Zhang, Xinghua; Wang, Shikui; He, Yang; Yang, Gengliang; Li, Beilei; Yang, Junjie; Lu, Yuejuan; Sun, Jiewei
Chinese Journal of Chemistry, 2011 , vol. 29, # 4 p. 757 - 764
反应条件
pyridine; quinoline; nickel dichloride
1 h; Heating;
参考文献
Gogia, Santosh; Sirohi, Reenu; Gupta, Suman; Kishore; Joshi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 1008 - 1011
反应条件
1: β-bromopropionic acid With potassium carbonate in ethanol; water
Schlenk techniqueInert atmosphere;
2: chlorophenyl mercaptan With potassium hydroxide in ethanol; water
Schlenk techniqueRefluxInert atmosphere;
参考文献
Grassi, David; Alexakis, Alexandre
Angewandte Chemie - International Edition, 2013 , vol. 52, # 51 p. 13642 - 13646
Angew. Chem., 2013 , vol. 125, # 51 p. 13887 - 13891,5
参考文献
Chu; Chang
Huaxue Xuebao, 1958 , vol. 24, p. 87,89
Chem.Abstr., 1959 , p. 7161
参考文献
Sen; Kulkarni
Journal of the Indian Chemical Society, 1957 , vol. 34, p. 687,689
