5-甲基-N-(三甲基硅烷基)-1,2-恶唑-3-胺合成路线 (共 2 条)
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 50, # 26 p. 5723 - 5727
反应条件
n-butyllithium
1.) THF, heptane, -70 deg C, 25 min, 2.) THF, heptane, from -70 deg C to RT, 1.5 h; Yield given. Multistep reaction;
参考文献
Sircar, Jagadish C.; Capiris, Thomas; Bobovski, Thomas P.; Schwender, Charles F.
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5723 - 5727