1-羟基-2,2,2-三氯乙基膦酸二乙酯合成路线 （共 15 条）
反应条件
water in benzene
T=80°C; 0.5 h;
参考文献
Ermanson, L. V.; Godovikov, N. N.; Blagoveshchenskii, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 395 - 396
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 427 - 429
反应条件
in benzene
T=40°C; Abramov reaction; 10 h; Inert atmosphere;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 428 - 433
反应条件
in Petroleum ether
T=-50°C;
参考文献
Gazizov, T. Kh.; Chugunov, Yu. V.; Abul'khanov, A. G.; Pudovik, A. N.
Doklady Chemistry, 1988 , vol. 298, p. 6 - 8
Dokl. Akad. Nauk SSSR Ser. Khim., 1988 , vol. 298, # 1 p. 112 - 115
反应条件
hydrogenchloride in diethyl ether
参考文献
Gazizov,T.Kh. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 10 p. 2383,2281 - 2282
反应条件
in Petroleum ether
temperature slowly brought from -40 deg C to r.t.; equimolar quantities of the educts;
参考文献
Gazizov, T. Kh.; Chugunov, Yu. V.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 3 p. 701 - 702,618 - 619
参考文献
Teichmann,B.
Journal fuer Praktische Chemie (Leipzig), 1965 , vol. 28, p. 94 - 98
反应条件
aluminum oxide
0.0666667 h; microwave irradiation;
参考文献
Javidan, Abdollah; Banan
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 11 p. 2253 - 2258
参考文献
Barthel et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 4186
反应条件
T=85°C; 0.5 h; Product distribution;
参考文献
Ermanson, L. V.; Godovikov, N. N.; Blagoveshchenskii, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 395 - 396
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 427 - 429
参考文献
Barthel et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 2424,2426
