2-氨基-4-硝基甲苯合成路线 (共 108 条)
反应条件
trimethylsilylazide; copper; ethanolamine in N,N-dimethyl acetamide T=95°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 6 p. 1712 - 1722
反应条件
1: With sulfuric acid T=-5°C; 2: With nitric acid T=-5°C; 2 h; 3: With sodium hydroxide in water Cooling with ice;
参考文献
Molecules, , vol. 14, # 10 p. 4166 - 4179
反应条件
nickel; hydrazine hydrate in ethanol; 1,2-dichloro-ethane T=50 - 60°C; 4 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 10 p. 3159 - 3164
反应条件
Pd(phen)2(OTf)2 in chlorobenzene T=135°C; P=45003.6 Torr; 2 h; Yield given;
参考文献
Chemical Communications, , # 2 p. 217 - 218
反应条件
Pd-Fe; hydrogen; silica gel in ethanol T=25°C; P=760 Torr; var. Pd/Fe ratio; Rate constantProduct distribution;
参考文献
Journal of Catalysis, , vol. 150, # 2 p. 356 - 367
反应条件
hydrogen in methanol T=36°C; P=760.051 Torr; 0.25 h;
参考文献
Russian Chemical Bulletin, , vol. 58, # 10 p. 2070 - 2076
反应条件
hydrogenchloride Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 1 p. 31 - 41
Zhurnal Organicheskoi Khimii, , vol. 27, # 1 p. 36 - 47
反应条件
sulfur dioxide; water; iron T=80 - 90°C;
参考文献
DE289454 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 119
反应条件
zinc(II) chloride in ethanol Heatingother N,N-dimethylformamidine and N-formyl derivatives; MechanismProduct distribution;
参考文献
Synthetic Communications, , vol. 24, # 11 p. 1617 - 1624
反应条件
sulfuric acid; nitric acid Verseifung der Acetylverbindung;
参考文献
Chemische Berichte, , vol. 17, p. 265