1,2-双(二苯基膦)乙烷一氧化物合成路线 （共 5 条）
反应条件
methyl-diethoxy-silane; di-p-nitrophenylphosphoric acid in toluene T=110°C; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yuehui; Lu, Liang-Qiu; Das, Shoubhik; Pisiewicz, Sabine; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2012 , vol. 134, # 44 p. 18325 - 18329
反应条件
palladium diacetate; sodium hydroxide; ethylene dibromide in 1,2-dichloro-ethane
7 h; Heating;
参考文献
Grushin, Vladimir V.
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5831 - 5832
反应条件
potassium tert-butylate in xylene
T=100°C; 6 h;
参考文献
Kabachnik, M. I.; Medved', T. Ya.; Pisareva, S. A.; Ignat'eva, T. I.; Lomakina, L. N.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 495 - 500
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 673 - 678
反应条件
1: With trifluoromethylsulfonic anhydride in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: With n-pentylmercaptane; N-ethyl-N,N-diisopropylamine in dichloromethane
T=20°C; 16 h; Inert atmosphere; Mechanism;
参考文献
Petersson, Maria J.; Loughlin, Wendy A.; Jenkins, Ian D.
Chemical Communications, 2008 , # 37 p. 4493 - 4494
反应条件
potassium hydroxide in dimethyl sulfoxide
T=85 - 90°C; 0.75 h;
参考文献
Bondarenko, N. A.; Rudomino, M. V.; Tsvetkov, E. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.2. p. 1989
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , vol. 39, # 9 p. 2180 - 2181
