alpha-苯基偶氮三苯基甲烷合成路线 (共 111 条)
参考文献
Wieland
Justus Liebigs Annalen der Chemie, 1934 , vol. 514, p. 145,157
反应条件
in acetonitrile Ambient temperature; Further byproducts given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 23, p. 111 - 142
反应条件
in tetrachloromethane 1.) heating, 30 h; 2.) 0 deg C, 48 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 711 - 716
反应条件
sodium methylate; 2,2-dimethoxy-propane 10 h; Heating; Mechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 491 - 498
参考文献
Justus Liebigs Annalen der Chemie, , vol. 514, p. 145,157
反应条件
in tetrachloromethane T=0°C; 20 h; Yields of byproduct given;
参考文献
Correa, Carlos M. M. da Silva; Oliveira, Maria Augusta B. C. S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 711 - 716
反应条件
in tetrachloromethane T=0°C; 2 h; Product distribution;
参考文献
Correa, Carlos M. M. da Silva; Oliveira, Maria Augusta B. C. S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 711 - 716
反应条件
triphenylphosphine in benzene T=60°C; Substitution; Isomerization; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 18 p. 1777 - 1778
反应条件
in toluene T=100°C; 1.45 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1338 - 1344
反应条件
p-methoxyphenylmagnesium bromide in toluene T=110°C; 0.833333 h; Schlenk technique;
参考文献
Uchiyama, Nanase; Shirakawa, Eiji; Hayashi, Tamio
Chemical Communications, 2013 , vol. 49, # 4 p. 364 - 366