反应条件
1: 2-bromo-2-phenyl-1-ethene With dichloro bis(acetonitrile) palladium(II); triethylamine; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane; biphenyl-2-yl-di-tert-butyl-phosphane in 1,4-dioxane
T=110°C; 4 h; Inert atmosphere;
2: 4'-iodoacetophenone With caesium carbonate in 1,4-dioxane; methanol
T=100°C; Suzuki Coupling; 20 h; Reagent/catalyst;
参考文献
Tasch, Boris O. A.; Bensch, Lisa; Antovic, Dragutin; Mueller, Thomas J. J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6113 - 6118
