环戊基(4-甲基苯基)甲酮合成路线 (共 7 条)
反应条件
(1,2,3,4-Me4-5-CF3-cyclopentadiene)Rh(CH2=CH-SiMe3)2 in toluene
T=75°C; 6 h;
参考文献
Roy, Amy H.; Lenges, Christian P.; Brookhart, Maurice
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 2082 - 2093
反应条件
1: in diethyl ether
T=0°C; Inert atmosphereReflux;
2: With hydrogenchloride; water; acetic acid in diethyl ether; water
参考文献
Cheng, Xu; Goddard, Richard; Buth, Gernot; List, Benjamin
Angewandte Chemie - International Edition, 2008 , vol. 47, # 27 p. 5079 - 5081
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran
T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran
T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
aluminum tri-bromide; 1,1-dibromomethane in tetrachloromethane
T=0°C;
参考文献
Akhrem; Churilova; Orlinkov; Afanas'eva; Vitt; Petrovskii
Russian Chemical Bulletin, 1998 , vol. 47, # 5 p. 918 - 923
反应条件
aluminum tri-bromide; 1,1-dibromomethane in tetrachloromethane
T=0°C;
参考文献
Akhrem; Churilova; Orlinkov; Afanas'eva; Vitt; Petrovskii
Russian Chemical Bulletin, 1998 , vol. 47, # 5 p. 918 - 923
反应条件
1.) ether; 2.) benzene, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Imai, Eiji; Iwamura, Tatsunori; Maeda, Kaori
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3599 - 3605