dipotassium N-cyano-dithioimidocarbonate in water T=25 - 30°C; 24 h;
参考文献
Ruminski, Peter G.; Suba, Lydia A.; D'Amico, John J.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 335 - 344
→
反应条件
1: 1,3-diphenyl-1,3-propanedione With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: C4H6N2SSe in tetrahydrofuran 2 h; Heating; Further stages. Further byproducts.;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 4 p. 613 - 616
→
反应条件
1: acetylacetone With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: C4H6N2SSe in tetrahydrofuran 2 h; Heating; Further stages. Further byproducts.;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 4 p. 613 - 616
→
反应条件
1: propionic anhydride With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: C4H6N2SSe in tetrahydrofuran 2 h; Heating; Further stages.;
