反-1,2-双(苯基磺酰基)乙烯合成路线 (共 19 条)
反应条件
iodine in dichloromethane Irradiation;
参考文献
Lucchi, Ottorino De; Lucchini, Vittorio; Pasquato, Lucia; Modena, Giorgio
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 596 - 604
反应条件
dihydrogen peroxide; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 75, p. 1672
Journal of the American Chemical Society, , vol. 76, p. 5745
Journal of the American Chemical Society, , vol. 81, p. 4927,4929
Gazzetta Chimica Italiana, , vol. 86, p. 428,431, 755
反应条件
in methanol; water 5 h; Ambient temperature;
参考文献
Reddy, D. Bhaskar; Babu, N. Chandrasekhar; Padmavathi; Sumathi
Synthesis, 1999 , # 3 p. 491 - 494
反应条件
in methanol; water 3 h; Ambient temperature;
参考文献
Reddy, D. Bhaskar; Babu, N. Chandrasekhar; Padmavathi; Sumathi
Synthesis, 1999 , # 3 p. 491 - 494
反应条件
1: 78 percent / Et3N / benzene / 18 h / 20 °C 2: methanol; H2O / 5 h / 20 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 42, # 2 p. 333 - 335
反应条件
tetrahydropyridine hydrochloride in xylene T=138°C; 3 h; var. catalysts; Product distribution;
参考文献
Naplyuev, V. M.; Bazavova, I. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1991 - 1992
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2231 - 2232
反应条件
1: 80 percent / AlCl3 / CHCl3 / 18 h / 55 - 65 °C 2: 78 percent / Et3N / benzene / 18 h / Ambient temperature 3: 80 percent / methanol; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 3 p. 491 - 494
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in toluene 2 h;
参考文献
Quintard, Adrien; Alexakis, Alexandre
Chemistry - A European Journal, 2009 , vol. 15, # 42 p. 11109 - 11113
反应条件
in N,N-dimethyl-formamide 1.) 14 deg C, 1 h; 2.) rt, 3h;
参考文献
Sepiol, Janusz; Soulen, Robert L.; Sepiol, Jadwiga
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 163 - 170
反应条件
sulfuric acid; dihydrogen peroxide 1.) flame distilled, 220-230 deg C, 14 Torr, 2.) glacial acetic acid, 0 deg C, 3.) 120 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 49, # 4 p. 596 - 604