顺-1,2-双(苯基磺酰基)乙烯合成路线 (共 15 条)
反应条件
dihydrogen peroxide in acetic acid 2 h; Heating;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Durr, Richard; Fabris, Fabrizio
Synthetic Communications, 1996 , vol. 26, # 2 p. 211 - 216
反应条件
1: ethanolic KOH 2: aqueous hydrogen peroxide; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 76, p. 5745
反应条件
1: 85 percent / sodium ethoxide / ethanol / 72 h / 110 °C 2: 95 percent / H2O2 / acetic acid / 2 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 26, # 2 p. 211 - 216
参考文献
Afarinkia, Kamyar; Mahmood, Farzana
Tetrahedron Letters, 2000 , vol. 41, # 8 p. 1287 - 1290
反应条件
iodine in dichloromethane Irradiation;
参考文献
Lucchi, Ottorino De; Lucchini, Vittorio; Pasquato, Lucia; Modena, Giorgio
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 596 - 604
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in toluene 2 h;
参考文献
Quintard, Adrien; Alexakis, Alexandre
Chemistry - A European Journal, 2009 , vol. 15, # 42 p. 11109 - 11113
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Benati, Luisa; Calestani, Gianluca; Nanni, Daniele; Spagnolo, Piero; Volta, Marco
Tetrahedron, 1997 , vol. 53, # 27 p. 9269 - 9278
反应条件
tri-n-butyl-tin hydride in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Durr, Richard; Fabris, Fabrizio
Synthetic Communications, 1996 , vol. 26, # 2 p. 211 - 216
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.0166667 h;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Durr, Richard; Fabris, Fabrizio
Synthetic Communications, 1996 , vol. 26, # 2 p. 211 - 216
反应条件
sodium hydride 1.) THF, 0 deg C, 20 min, 2.) THF, 0 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Cossu, Sergio; De Lucchi, Ottorino; Fabris, Fabrizio; Ballini, Roberto; Bosica, Giovanna
Synthesis, 1996 , # 12 p. 1481 - 1484