反应条件
methanol; water in tetrahydrofuran; hexane; benzene
Kinetics; vac.; addn. of MeOH in THF/benzene to Ge-compound in THF (-78°C), after 5 min addn. of Me3SiCl, stirring (room temp., 1 h), addn. of water and hexane; sepn. of org. layer, drying (MgSO4); GLC anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Voronkov, M. G.; Vyazankin, N. S.
Journal of General Chemistry USSR (English Translation), 1989 , vol. 59, p. 761 - 763
Zhurnal Obshchei Khimii, 1989 , vol. 59, p. 863 - 865
