N-(5-溴戊基)邻苯二甲酰亚胺合成路线 （共 34 条）
反应条件
tetrabutylammomium bromide in acetonitrile 20 h; Reflux;
参考文献
Ignasik, Michalina; Bajda, Marek; Guzior, Natalia; Prinz, Michaela; Holzgrabe, Ulrike; Malawska, Barbara
Archiv der Pharmazie, 2012 , vol. 345, # 7 p. 509 - 516
反应条件
potassium carbonate in N,N-dimethyl-formamide 72 h; Ambient temperature;
参考文献
Constant; Carden; Lhomme
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 4 p. 1035 - 1040
反应条件
phosphorus tribromide in diethyl ether
参考文献
Kaken Pharmaceutical Co., Ltd.
Patent: US6255321 B1, 2001 ;
反应条件
bromine; triphenylphosphine in dichloromethane; toluene
参考文献
US5654431 A1, ;
US 5654431 A
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Kowalski, Piotr; Mitka, Katarzyna; Jaskowska, Jolanta; Duszynska, Beata; Bojarski, Andrzej J.
Archiv der Pharmazie, 2013 , vol. 346, # 5 p. 339 - 348
反应条件
in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide
反应条件
in N-methyl-acetamide; water
参考文献
US5302593 A1, ;
US 5302593 A
参考文献
Merck and Co., Inc.
Patent: US4705892 A1, 1987 ;
US 4705892 A
反应条件
1: 90 percent / dimethylformamide / 16 h / 20 °C 2: K2CO3; MeOH / 20 °C 3: PPh3; CBr4 / acetonitrile / 16 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 19 p. 3175 - 3186
反应条件
1: K2CO3; MeOH / 20 °C 2: PPh3; CBr4 / acetonitrile / 16 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 19 p. 3175 - 3186
