2,3,5,6-四溴-4-甲基-4-硝基-2,5-环己二烯-1-酮合成路线 (共 8 条)
反应条件
nitric acid; acetic anhydride T=0 - 20°C; 0.166667 h;
参考文献
Arnatt, Christopher K.; Zhang, Yan
Tetrahedron Letters, 2012 , vol. 53, # 13 p. 1592 - 1594
反应条件
1: 81 percent / Br2 / iron dust / CCl4 / 1.) 5 h bromine introduction; 2.) 24 h room temp. 2: 88 percent / nitric acid / acetic acid / 1.) 10 min 10 deg C; 2.) 2 h 5 deg C View Scheme
参考文献
Tetrahedron, , vol. 43, # 5 p. 835 - 844
反应条件
in diethyl ether T=20°C; further solvents, temp. effect, nitration of further substituted naphthols, further nitrocyclohexadienones; Product distribution;
参考文献
Lemaire, Marc; Guy, Alain; Roussel, Jacques; Guette, Jean-Paul
Tetrahedron, 1987 , vol. 43, # 5 p. 835 - 844
反应条件
in diethyl ether T=20°C; further solvents, temp. effect, nitration of further substituted naphthols, further nitrocyclohexadienones; Product distribution;
参考文献
Lemaire, Marc; Guy, Alain; Roussel, Jacques; Guette, Jean-Paul
Tetrahedron, 1987 , vol. 43, # 5 p. 835 - 844
反应条件
in acetone T=-50 - 30°C; phenol; Mechanism;
参考文献
Coombes, Robert G.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 7 p. 1007 - 1008
反应条件
in diethyl ether T=20°C; further solvents, temp. effect, nitration of further substituted naphthols, further nitrocyclohexadienones; Product distribution;
参考文献
Lemaire, Marc; Guy, Alain; Roussel, Jacques; Guette, Jean-Paul
Tetrahedron, 1987 , vol. 43, # 5 p. 835 - 844
参考文献
Zincke; Buff
Justus Liebigs Annalen der Chemie, 1905 , vol. 341, p. 347
反应条件
in acetone T=-50 - 30°C; phenol; Mechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1007 - 1008