2-脱氧-2,2-二氟-D-赤式戊呋喃酮糖-3,5-二醇合成路线 （共 9 条）
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C;
参考文献
CHEMAGIS LTD.
Patent: US2007/191598 A1, 2007 ;
Location in patent: Page/Page column 14 ;
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C;
参考文献
CHEMAGIS LTD.
Patent: US2007/191598 A1, 2007 ;
Location in patent: Page/Page column 13-14 ;
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C; 370 h;
参考文献
CHEMAGIS LTD.
Patent: US2007/191598 A1, 2007 ;
Location in patent: Page/Page column 13 ;
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=20 - 60°C; 6.16667 h;
参考文献
CHEMAGIS LTD.
Patent: US2007/191598 A1, 2007 ;
Location in patent: Page/Page column 12-13 ;
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C; 6.25 h;
参考文献
CHEMAGIS LTD.
Patent: US2007/191598 A1, 2007 ;
Location in patent: Page/Page column 13 ;
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C; 6.25 h;
参考文献
US2007/191598 A1, ;
Page/Page column 13 ;
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in ethyl acetate T=60 - 65°C; 6 h; Product distribution / selectivity;
参考文献
WO2005/95430 A1, ;
Page/Page column 7; 13; 15 ;
反应条件
Multi-step reaction with 3 steps 1: 2,6-lutidine / CH2Cl2 2: diisobutylaluminium hydride / toluene / 2 h / -64 °C3: 79 percent / HBr gas / CH2Cl2 / 12 h / Ambient temperature
参考文献
Hertel; Kroin; Misner; Tustin Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2406 - 2409
反应条件
Multi-step reaction with 3 steps 1: 2,6-lutidine / CH2Cl2 2: diisobutylaluminium hydride / toluene / 2 h / -64 °C3: 90 percent / triethylamine / CH2Cl2 / 3 h / 25 °C
参考文献
Hertel; Kroin; Misner; Tustin Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2406 - 2409
