1,2,4,5-四氯苯合成路线 (共 206 条)
反应条件
potassium hydroxide; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride; palladium diacetate in 1,4-dioxane T=95°C; Suzuki coupling;
参考文献
Russian Chemical Bulletin, , vol. 56, # 7 p. 1467 - 1469
反应条件
potassium methanolate; bis(dibenzylideneacetone)-palladium(0) in methanol; toluene T=95°C; Suzuki coupling;
参考文献
Russian Chemical Bulletin, , vol. 56, # 7 p. 1467 - 1469
反应条件
T=25°C; 40 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3122 - 3126
反应条件
potassium 1) HMPA, 20 deg C; 2) 110 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.; Rembovskii, V. R.; Troshkin, N. M.; Baulin, S. I.
Doklady Chemistry, 1993 , vol. 332, # 4 p. 225 - 229
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 332, # 4 p. 461 - 465
反应条件
1: carbon dioxide With [Au(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)hydroxide]; potassium hydroxide in tetrahydrofuran T=20°C; P=1125.11 Torr; 0.25 h; 2: 1,2,4,5-TeCB in tetrahydrofuran T=20°C; P=1125.11 Torr; 12 h; 3: With hydrogenchloride in tetrahydrofuran; water regioselective reaction;
参考文献
Boogaerts, Ine I. F.; Nolan, Steven P.
Journal of the American Chemical Society, 2010 , vol. 132, # 26 p. 8858 - 8859
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Uhlenbroek,J.H.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 1057 - 1065
反应条件
T=25°C; 40 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3122 - 3126
反应条件
D2SO4 (sulfonic acid-d2) T=150°C;
参考文献
Saeki; Leitch
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 249, p. 2307
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 24 h; Heating;
参考文献
Burukin; Vasil'ev; Chizhov; Zlotin
Russian Chemical Bulletin, 2005 , vol. 54, # 4 p. 970 - 974
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.5 h; Aliquat 336 and other phase-transfer catalysts, different multiphase systems, different time and solvents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5256 - 5260