暂无反应条件数据

暂无反应条件数据

18-crown-6 ether; oxygen; potassium carbonate in water T=80°C; P=760.051 Torr; 10 h;

1: potassium hydroxide; [bis(acetoxy)iodo]benzene / 3 h / 0 °C 2: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux 3: potassium carbonate; 18-crown-6 ether; oxygen / water / 10 h / 80 °C / 760.05 Torr View Scheme

1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux 2: potassium carbonate; 18-crown-6 ether; oxygen / water / 10 h / 80 °C / 760.05 Torr View Scheme

T=120 - 125°C;