3,4-亚甲基二氧基苯硼酸频那醇酯合成路线 （共 14 条）
反应条件
triethylamine; 1,2-bis[(diphenylarsino)]ethane; palladium diacetate in 1,4-dioxane T=80°C; 24 h;
参考文献
Commonwealth Scientific and Industrial Research Organisation
Patent: US6680401 B1, 2004 ;
Location in patent: Page column 26 ;
反应条件
1: 1,2-methylenedioxy-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Inert atmosphere; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane T=-78°C; Inert atmosphere;
参考文献
Ebner, David C.; Bagdanoff, Jeffrey T.; Ferreira, Eric M.; McFadden, Ryan M.; Caspi, Daniel D.; Trend, Raissa M.; Stoltz, Brian M.
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 12978 - 12992
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 3 h; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 3 h; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
反应条件
in dimethyl sulfoxide T=20°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 54, # 2 p. 166 - 169
反应条件
[Ir2(OMe)2(1,5-cyclooctadiene)2]; 2,2'-bis(2-oxazoline) in cyclohexane T=70°C; 24 h; Inert atmosphere;
参考文献
Vanchura II, Britt A.; Preshlock, Sean M.; Roosen, Philipp C.; Kallepalli, Venkata A.; Staples, Richard J.; Maleczka Jr., Robert E.; Singleton, Daniel A.; Smith III, Milton R.
Chemical Communications, 2010 , vol. 46, # 41 p. 7724 - 7726
反应条件
tert.-butylnitrite in acetonitrile T=80°C; 2 h;
参考文献
Qiu, Di; Jin, Liang; Zheng, Zhitong; Meng, He; Mo, Fanyang; Wang, Xi; Zhang, Yan; Wang, Jianbo
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1923 - 1933
反应条件
1: in tetrahydrofuran; hexane T=20°C; 2 h; 2: With acetic acid in tetrahydrofuran; hexane T=20°C; 18 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 4 p. 1026 - 1035
反应条件
1: C13H20BNO2 With methanol in ethyl acetate T=-5 - 20°C; 1 h; Inert atmosphereSchlenk technique; 2: 2,3-dimethylbutane-2,3-diol in diethyl ether T=20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Guerrand, Helene D. S.; Marciasini, Ludovic D.; Jousseaume, Melissa; Vaultier, Michel; Pucheault, Mathieu
Chemistry - A European Journal, 2014 , vol. 20, # 19 p. 5573 - 5579
反应条件
1: triethylamine / dichloromethane 2: potassium acetate / tert-butyl alcohol / 3 h / 90 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
