2-氰基-6-甲氧基苯并噻唑合成路线 (共 21 条)
反应条件
pyridine; 1H-imidazole; trichlorophosphate in dichloromethane T=-10 - 20°C; Inert atmosphere;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
copper(l) iodide; tetrabutylammomium bromide; palladium dichloride in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; 3 h; Inert atmosphere;
参考文献
McCutcheon, David C.; Paley, Miranda A.; Steinhardt, Rachel C.; Prescher, Jennifer A.
Journal of the American Chemical Society, 2012 , vol. 134, # 18 p. 7604 - 7607
反应条件
1: (i) P2S5, xylene, (ii) K3<Fe(CN)6>, aq. NaOH 2: HCl 3: NH3 / methanol 4: POCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 85, p. 337 - 343
反应条件
1: HCl 2: NH3 / methanol 3: POCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 85, p. 337 - 343
反应条件
1: NH3 / methanol 2: POCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 85, p. 337 - 343
反应条件
in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Xie, Aming; Cao, Meiping; Liu, Yangyang; Feng, Liandong; Hu, Xinyu; Dong, Wei
European Journal of Organic Chemistry, 2014 , vol. 2014, # 2 p. 436 - 441
反应条件
in dimethyl sulfoxide T=110°C; 5 h;
参考文献
Suzuki, Nobutaka; Nomoto, Tateo; Toya, Yoshiaki; Kanamori, Norio; Yoda, Binkoh; Saeki, Akio
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 9 p. 1561 - 1562
反应条件
in dimethyl sulfoxide T=110°C; 5 h;
参考文献
Meroni, Giuseppe; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Synlett, 2009 , # 16 p. 2682 - 2684
反应条件
1: 79.3 percent / CuBr2, isoAmONO, polyethylene glycol / acetonitrile / 3 h / 50 °C 2: 70.4 percent / dimethylsulfoxide / 5 h / 110 °C View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 57, # 9 p. 1561 - 1562
反应条件
in dimethyl sulfoxide T=110°C; 10 h;
参考文献
Suzuki, Nobutaka; Nomoto, Tateo; Toya, Yoshiaki; Kanamori, Norio; Yoda, Binkoh; Saeki, Akio
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 9 p. 1561 - 1562