1,3-二苯基-1H-吡唑-5-羧酸乙酯合成路线 (共 7 条)
反应条件
in methanol
T=65°C; TemperatureSolvent; regiospecific reaction;
参考文献
Zhu, Huajian; Shao, Nana; Chen, Tong; Zou, Hongbin
Chemical Communications, 2013 , vol. 49, # 70 p. 7738 - 7740
反应条件
1: 96.4 percent / Na; EtOH / toluene
2: 46.2 percent / ethanol / 3 h / Heating
View Scheme
参考文献
Schmidt, Andreas; Habeck, Tobias; Kindermann, Markus Karl; Nieger, Martin
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5977 - 5982
反应条件
in ethanol
3 h; Heating;
参考文献
Schmidt, Andreas; Habeck, Tobias; Kindermann, Markus Karl; Nieger, Martin
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5977 - 5982
反应条件
sulfuric acid in ethanol; water
1 h; Heating; Yield given. Yields of byproduct given;
参考文献
Begtrup, Mikael; Vedso, Per; Cabildo, Pilar; Claramunt, Rosa Maria; Elguero, Jose; Meutermans, Wim
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 5 p. 455 - 459
反应条件
sulfuric acid
T=20°C; Reflux;
参考文献
Yang, Xueyan; Shui, Shengxia; Chen, Xi; He, Hai'ou; Wu, Fanhong
Journal of Fluorine Chemistry, 2010 , vol. 131, # 3 p. 426 - 432
反应条件
4 h; Heating; Yield givenYields of byproduct given;
参考文献
Martins, Marcos A. P.; Freitag, Rogerio A.; Da Rosa, Adriano; Flores, Alex F. C.; Zanatta, Nilo; Bonacorso, Helio G.
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 217 - 220
参考文献
Begtrup, Mikael; Vedso, Per; Cabildo, Pilar; Claramunt, Rosa Maria; Elguero, Jose; Meutermans, Wim
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 5 p. 455 - 459