1-溴-3,5-二甲基金刚烷合成路线 （共 25 条）
反应条件
1: H2SO4, BF3 2: Br2 3: H2SO4 / 6 h / Heating 4: H2SO4, BF3 5: H2SO4 / 5 h / Heating View Scheme
参考文献
Bott,K.
Chemische Berichte, 1968 , vol. 101, p. 564 - 573
反应条件
2,2'-azo-bisisobutyronitrile; α,α,α-trifluorotoluene; (C6F13CH2CH2)3SnH; sodium cyanoborohydride in tert-butyl alcohol T=90°C; P=60800 Torr; 3 h;
参考文献
Ryu, Ilhyong; Niguma, Tatsuro; Minakata, Satoshi; Komatsu, Mitsuo; Hadida, Sabine; Curran, Dennis P.
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7883 - 7886
反应条件
1: H2SO4 2: KOH View Scheme
参考文献
Shanghai Institute of Pharmaceutical Industry; Zhejiang Kangyu Pharmaceutical Co., Ltd.
Patent: EP1674446 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;
参考文献
Ren, Huixue; Ying, Hanjie; Ouyang, Pingkai; Lin, Jimao; Jing, Liu
Asian Journal of Chemistry, 2012 , vol. 24, # 11 p. 5107 - 5110
反应条件
T=25 - 140°C; 3 - 5 h; Product distribution / selectivity;
参考文献
CADILA HEALTHCARE LIMITED
Patent: WO2008/62472 A2, 2008 ;
Location in patent: Page/Page column 13-17 ;
