4-(4-甲基-1-哌嗪甲基)苯硼酸频哪酯合成路线 （共 7 条）
反应条件
sodium acetate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Inert atmosphereReflux;
参考文献
WO2012/119941 A1, ;
Page/Page column 116 ;
WO 2012/119941 A1
反应条件
PS-NMM in tetrahydrofuran T=150°C; 0.583333 h; Microwave irradiationin air;
参考文献
ACS Combinatorial Science, , vol. 13, # 1 p. 24 - 31
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C 2: sodium acetate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux View Scheme
参考文献
WO2012/119941 A1, ;
WO 2012/119941 A1
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C 2: sodium acetate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux View Scheme
参考文献
WO2012/119941 A1, ;
WO 2012/119941 A1
