2,2,2-三甲基苯乙酮合成路线 (共 203 条)
参考文献
Journal of the American Chemical Society, , vol. 103, p. 4494
反应条件
1: 2.) 2 N aq. HCl / 1.) CH3OH, reflux, 6 h, 2.) room temperature, 2 days 2: 1.) NaNH2 / 1.) toluene, reflux, 2 h, 2.) reflux, 2-10 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 11 p. 2587 - 2590
反应条件
1: 2.) 2 N aq. HCl / 1.) CH3OH, reflux, 4 h, 2.) room temperature, 2 days 2: 1.) NaNH2 / 1.) toluene, reflux, 2 h, 2.) reflux, 2-10 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 11 p. 2587 - 2590
参考文献
Journal of Organic Chemistry, , vol. 48, # 7 p. 1144 - 1146
反应条件
magnesium 1.) ether, 2.) ether, -15 deg C; Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 3 p. 856 - 866
反应条件
sodium amide 1.) toluene, reflux, 2 h, 2.) reflux, 2-10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 11 p. 2587 - 2590
反应条件
in xylene 12 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 183 - 187
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 148, p. 73
反应条件
3,3-dimethyldioxirane in acetone T=25°C; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 77, # 3 p. 308 - 312
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 1 p. 157 - 161