in toluene
Irradiation (UV/VIS); (Ar); dissolving of Et3SiH and Ge3(C6H2Me3)6 in toluene, irradn. (350 nm) at -70°C for 18 h; addn. via cannula of soln. m-chloroperbenzoic acid in dried degassed toluene; washing with satd. Na2SO3 and then with water, removal of solvent under vac., sepn. by chromy. (90/10 CH2Cl2-hexane);
参考文献
Samuel, Mini S.; Jennings, Michael C.; Baines, Kim M.
Journal of Organometallic Chemistry, 2001 , vol. 636, # 1-2 p. 130 - 137