三甲基(3-甲基苯基)锡烷合成路线 (共 39 条)
反应条件
palladium diacetate in diethyl ether; acetonitrile 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
反应条件
aluminium trichloride in dichloromethane T=-30°C; 2 h; Yield given;
参考文献
Tetrahedron, , vol. 45, # 4 p. 951 - 960
反应条件
iodine in methanol Kinetics; byproducts: m-CH3C6H4I; mechanism discussed;;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 72, p. 286 - 288
Helvetica Chimica Acta, , vol. 47, p. 1679 - 1687
反应条件
ArPdI(P(C6H5)3)2 in 1,2-dichloro-ethane T=120 - 130°C; 2 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, , vol. 17, # 1 p. 21 - 28
反应条件
palladium diacetate in water; acetonitrile T=20°C; 2 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 10 p. 1605 - 1609
Zhurnal Organicheskoi Khimii, , vol. 30, # 10 p. 1524 - 1527
反应条件
trichlorophosphate T=50 - 70°C; 3 h;
参考文献
Tetrahedron, , vol. 45, # 4 p. 951 - 960
反应条件
in dichloromethane byproducts: m-CH3C6H4CN; in presence of AlCl3;;
参考文献
Journal of Organometallic Chemistry, , vol. 46, p. 267
Journal of the Chemical Society [Section] C: Organic, , p. 1717 - 1718
C. A., U.S. Clearinghouse Fed. Sci. Tech. Inform. AD 701102 (1969)11 S. , vol. 73, p. 35473
反应条件
in not given byproducts: m-CH3C6H4NO;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1717 - 1718
C. A., U.S. Clearinghouse Fed. Sci. Tech. Inform. AD 701102 (1969)11 S. , vol. 73, p. 35473
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; Stille coupling; 0.5 h; Sonication;
参考文献
Domini, Claudia E.; Silbestri, Gustavo F.; Fernandez Band, Beatriz; Chopa, Alicia B.
Ultrasonics Sonochemistry, 2012 , vol. 19, # 3 p. 410 - 414
反应条件
in dichloromethane T=120 - 130°C; P=0.001 Torr; 2 h; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, , vol. 20, # 3 p. 457 - 464