反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1.1: 3.15 g / potassium hydroxide / H<sub>2</sub>O; methanol / 12 h / 20 °C<br />2.1: 28 percent / LiAlH<sub>4</sub> / tetrahydrofuran / 1 h / 0 - 20 °C<br />3.1: 85 percent / pyridinium chlorochromate / CH<sub>2</sub>Cl<sub>2</sub> / 3 h / 20 °C<br />4.1: triphenylphosphine; zinc / CH<sub>2</sub>Cl<sub>2</sub> / 20 h / 20 °C<br />4.2: 93 percent / CH<sub>2</sub>Cl<sub>2</sub> / 20 h / 20 °C<br /> <br />
参考文献
Schmittel, Michael; Mahajan, Atul A.; Bucher, Goetz; Bats, Jan W. Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2166 - 2173
