Gerrard,W. et al.
Journal of the Chemical Society, 1962 , p. 113 - 119
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Gmelin Handbook: B: B-Verb.4, 4.4.2.3.3, page 126 - 130
in toluene
refux under BCl3 for 6 h, cooling to 20°C, standing 3 d; crystn., filtration, drying (vac.), isolation of borazine by evapn.;
参考文献
Avent, Anthony G.; Hitchcock, Peter B.; Lappert, Michael F.; Liu, Dian-Sheng; Mignani, Gerard; et al.
Journal of the Chemical Society, Chemical Communications, 1995 , # 8 p. 855 - 856
in neat (no solvent)
byproducts: Me3SiBr; heating chloro- and bromoborazine (150°C, 1 h); volatiles removed (40°C, vac.); distn. of gummy residue at 30-36°C (1 Torr) left glassy residue, identification of distillate (mass spectroscopy, (11)B NMR) as mixt. of chloroborazines;
参考文献
Niedenzu, Kurt; Serwatowska, Joanne; Serwatowski, Janusz
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 5 p. 713 - 717
