1.1: NEt3; MsCl; DMAP / CH2Cl2 / 36 h / 0 - 20 °C 1.2: 3380 mg / aq. H2SO4 / CH2Cl2 / 48 h / 20 °C 2.1: 77 percent / H2 / Pd(OH)2/C / ethanol; ethyl acetate / 14 h / 20 °C / 760 Torr 3.1: aq. HCl / 10 h / Heating 3.2: 92 percent / propylene oxide / ethanol / 5 h / 20 °C View Scheme

1.1: NEt3; MsCl; DMAP / CH2Cl2 / 36 h / 0 - 20 °C 1.2: 3380 mg / aq. H2SO4 / CH2Cl2 / 48 h / 20 °C 2.1: 77 percent / H2 / Pd(OH)2/C / ethanol; ethyl acetate / 14 h / 20 °C / 760 Torr View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098214', constants.ctx, '0')">hydrogenchloride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;<br /> &nbsp;