triethylamine in tetrahydrofuran soln. of borane in THF syringed onto 3-hexyne (-65°C, under N2), slowly warmed to room temp. , addn. of triethylamine (at room temp.), stirred (several days), monitored by (11)B NMR; repeated trap-to-trap distn., carborane remaining in the 0°C trap;
参考文献
Cendrowski-Guillaume, Sophie M.; Spencer, James T.
Organometallics, 1992 , vol. 11, p. 969 - 972
Barluenga, Jose; Martinez-Gallo, Jose M.; Najera, Carmen; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1017 - 1020
