methanol in neat (no solvent) Ar atmospher; addn. of MeOH to (Me2N)2BCCOEt (dropwise, water-cooling), heating (50-60°C, 1 h); fractionation (trap, solid carbon dioxide-cooling); NMR- and IR-spectroscopy;
参考文献
Ponomarev, S. V.; Gromova, E. M.; Nikolaeva, S. N.; Zolotareva, A. S.
Journal of General Chemistry USSR (English Translation), 1989 , vol. 59, p. 2040 - 2045
Zhurnal Obshchei Khimii, 1989 , vol. 59, p. 2277 - 2282
Burilov, A. R.; Cherepashkin, D. V.; Pudovik, M. A.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.1 p. 20 - 21
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 26 - 27