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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
92013-22-4
合成路线
（共 10 条）
2396-63-6
1,6-庚二炔
+
693-02-7
1-己炔
→
反应条件
92013-22-4
反应条件
tris (triphenylphosphine)rhodium(I) chloride in ethanol T=60°C; 2 h;
参考文献
Grigg, Ronald; Scott, Ronald; Stevenson, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1357 - 1364
92013-20-2
→
反应条件
92013-22-4
反应条件
hydrogen; platinum(IV) oxide in tetrahydrofuran P=1034.3 Torr; Yield given;
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
1643-30-7
3-(4-溴苯基)丙酸
→
反应条件
92013-22-4
反应条件
1: thionyl chloride 2: 91 percent / AlCl3 / CS2 3: 89 percent / NaBH4 / ethanol / 25 °C 4: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 5: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 6: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
70146-78-0
2-(4-溴苄基)-丙二酸二乙酯
→
反应条件
92013-22-4
反应条件
1: 95 percent / KOH / acetic acid; H2O; tetrahydrofuran 2: 85 percent / 165 °C 3: thionyl chloride 4: 91 percent / AlCl3 / CS2 5: 89 percent / NaBH4 / ethanol / 25 °C 6: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 7: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 8: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
14548-39-1
6-溴茚酮
→
反应条件
92013-22-4
反应条件
1: 89 percent / NaBH4 / ethanol / 25 °C 2: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 3: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 4: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
75476-86-7
6-溴-2,3-二氢-1H-茚-1-醇
→
反应条件
92013-22-4
反应条件
1: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 2: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 3: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
92013-18-8
2-(4-溴苄基)-丙二酸
→
反应条件
92013-22-4
反应条件
1: 85 percent / 165 °C 2: thionyl chloride 3: 91 percent / AlCl3 / CS2 4: 89 percent / NaBH4 / ethanol / 25 °C 5: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 6: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 7: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
75476-78-7
5-溴-1H-茚
→
反应条件
92013-22-4
反应条件
1: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 2: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
55394-81-5
3-(4-溴苯基)丙酰氯化
→
反应条件
92013-22-4
反应条件
1: 91 percent / AlCl3 / CS2 2: 89 percent / NaBH4 / ethanol / 25 °C 3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 4: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 5: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
589-15-1
对溴溴苄
→
反应条件
92013-22-4
反应条件
1: 74 percent / NaOEt / Heating 2: 95 percent / KOH / acetic acid; H2O; tetrahydrofuran 3: 85 percent / 165 °C 4: thionyl chloride 5: 91 percent / AlCl3 / CS2 6: 89 percent / NaBH4 / ethanol / 25 °C 7: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating 8: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating 9: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
