邻甲氧基-N-乙酰乙酰苯胺合成路线 （共 16 条）
反应条件
N,N'-bis(2-aminoethyl)ethane-1,2-diamine
反应条件
in xylene T=120°C; 0.5 h;
参考文献
Avendano; De la Cuesta; Gesto
Synthesis, 1991 , # 9 p. 727 - 730
参考文献
Maiti, Arup; Reddy, P. V. Narasimha; Sturdy, Megan; Marler, Laura; Pegan, Scott D.; Mesecar, Andrew D.; Pezzuto, John M.; Cushman, Mark
Journal of Medicinal Chemistry, 2009 , vol. 52, # 7 p. 1873 - 1884
参考文献
US2152787 , ;
US2152786 , ;
反应条件
in toluene 24 h; RefluxInert atmosphere;
参考文献
Wang, Min; Gao, Mingzhang; Miller, Kathy D.; Sledge, George W.; Hutchins, Gary D.; Zheng, Qi-Huang
Steroids, 2010 , vol. 75, # 12 p. 967 - 973
反应条件
in tetrahydrofuran 5 h; Photolysis;
参考文献
Photochemistry and Photobiology, , vol. 80, # 2 p. 175 - 184
反应条件
1: 99 percent / K2CO3 / dimethylformamide / 11 h / 20 °C 2: 33 percent / SnCl4; H2O / xylene / 4.5 h / 120 °C View Scheme
参考文献
Zhang, Zhiguo; Zhang, Qian; Sun, Shaoguang; Xiong, Tao; Liu, Qun
Angewandte Chemie - International Edition, 2007 , vol. 46, # 10 p. 1726 - 1729
反应条件
1: 2-methoxy-4nitro-aniline With hydrogenchloride; C19H23N7O8S3; sodium nitrite in water T=10°C; 1 h; 2: aceto-acetyl-amino-2-methoxy-benzene With sodium hydroxide; sodium acetate; acetic acid in water T=25 - 90°C; pH=6; 2.5 h;
参考文献
Sanyo Color Works, Ltd.
Patent: EP1424370 A1, 2004 ;
Location in patent: Page 10-11 ;
反应条件
1: o-tolidine-6,6'-disulfonic acid; 2-methoxy-4nitro-aniline With hydrogenchloride; sodium nitrite in water T=10°C; 1 h; 2: aceto-acetyl-amino-2-methoxy-benzene With sodium hydroxide; sodium acetate; acetic acid in water T=25 - 90°C; pH=6; 150 h;
参考文献
Sanyo Color Works, Ltd.
Patent: EP1424370 A1, 2004 ;
Location in patent: Page 10 ;
