1: With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-78°C; 2 h; Inert atmosphere; 2: With triethylamine in dichloromethane T=-78 - 20°C; Inert atmosphere;
参考文献
Zhu, Hai; Wickenden, Jason G.; Campbell, Natalie E.; Leung, Joe C. T.; Johnson, Kayli M.; Sammis, Glenn M.
Organic Letters, 2009 , vol. 11, # 9 p. 2019 - 2022
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane
8 h; Ambient temperature;
参考文献
Gillard, John W.; Fortin, Rejean; Morton, Howard E.; Yoakim, Christiane; Quesnelle, Claude A.; at al.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2602 - 2608