3,3-二甲基-1-丁炔合成路线 （共 306 条）
反应条件
18-crown-6 ether; potassium tert-butylate in Petroleum ether T=60°C; 2 h;
参考文献
Dehmlow, Eckehard V.; Lissel, Manfred
Liebigs Annalen der Chemie, 1980 , # 1 p. 1 - 13
反应条件
18-crown-6 ether; potassium tert-butylate in Petroleum ether T=60°C; 2 h;
参考文献
Dehmlow, Eckehard V.; Lissel, Manfred
Liebigs Annalen der Chemie, 1980 , # 1 p. 1 - 13
反应条件
methyllithium in tetrahydrofuran T=-30 - 0°C; Dehalogenation; 1 h;
参考文献
Wang, Zhe; Fortunak, Joseph M.
Patent: US6359164 B1, 2002 ;
Location in patent: Page column 13, 15-16 ;
反应条件
potassium hydroxide; tetra-n-octylammonium bromide in Petroleum ether T=90°C; 8 h;
参考文献
Dehmlow, Eckehard V.; Lissel, Manfred
Tetrahedron, 1981 , vol. 37, p. 1653 - 1658
反应条件
nonafluoro-n-butanesulfonyl fluoride; 1-tert-butyl-2,2,4,4,4-pentakis(dimethylamino)-25,45-catenodi(phosphazene) in 1-methyl-pyrrolidin-2-one T=-10 - 20°C;
参考文献
Lyapkalo, Ilya M.; Vogel, Michael A. K.; Boltukhina, Ekaterina V.; Vavrik, Jiri
Synlett, 2009 , # 4 p. 558 - 561
反应条件
T=750°C; P=0.01 Torr; 3 h;
参考文献
Aitken, R. Alan; Atherton, J. Ian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1281 - 1284
反应条件
potassium hydroxide; 2,3-dimethylbutane-2,3-diol; Aliquatreg; 336 in Petroleum ether 1.5 h; Heating;
参考文献
Verkruijsse, H.D.; Brandsma, L.
Synthetic Communications, 1990 , vol. 20, # 21 p. 3355 - 3358
反应条件
potassium hydroxide; ethanol; mineral oil T=200°C;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1611,1613
反应条件
potassium hydroxide; water in 1,3,5-trimethyl-benzene distillation;
参考文献
Fedenok, L. G.; Shvartsberg, M. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2376 - 2377
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2622 - 2624
反应条件
methyllithium in tetrahydrofuran T=-30 - 0°C; Elimination; 1 h;
参考文献
Wang, Zhe; Yin, Jianguo; Campagna, Silvio; Pesti, Jaan A.; Fortunak, Joseph M.
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6918 - 6920
