3-(叔丁基二甲基硅氧基)戊二酸二乙酯合成路线 （共 5 条）
反应条件
1H-imidazole in dichloromethane Inert atmosphere;
参考文献
Ivsic, Trpimir; Dokli, Irena; Rimac, Ana; Hamersak, Zdenko
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 631 - 638
参考文献
US5049577 A1, ;
US 5049577 A
参考文献
Journal of the American Chemical Society, , vol. 108, # 8 p. 1969 - 1979
反应条件
1: 1) NaOH 2) Ac2O / 1) MeOH, r.t. 2) benzene, 1.5h, reflux (better yield by using the di-K-salt of cpd.12 on a small scale basis) 2: Na / 1 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3657 - 3659
反应条件
sodium hydroxide; acetic anhydride in methanol; diethyl ether; benzene
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4804770 A1, 1989 ;
