hydrogen; carbon monoxide; Sn; silica gel in chlorobenzene T=96.9°C; P=12751 Torr; 4 h;
参考文献
Tret'yakov, V. P.; Zimtseva, G. P.; Chudaev, V. V.; Rudakov, E. S.; Ponomarev, V. N.; Kharchenko, T. P.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 948 - 951,867 - 870
1: With water; palladium diacetate; caesium carbonate; sodium thiosulfate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene; tert-butyl alcohol T=80°C; 24 h; Inert atmosphere; 2: With hydrogenchloride; zinc in water 1 h; Cooling with ice;
