反应条件
1: 1.) magnesium / 1.) THF, reflux, 1.5 h., 2.) benzene, THF, room temp., 2 h.
3: diisobutylaluminum hydride / diethyl ether / 0.5 h / -105 - -95 °C
4: diethyl zinc, O2 / toluene / 0.17 h
5: Celite, pyridinium chlorochromate / CH2Cl2 / 1.5 h / Ambient temperature
6: benzene / 2.25 h / Ambient temperature
View Scheme
参考文献
Gadwood,R.C.; Lett,R.M.; Wissinger,J.E.
Journal of the American Chemical Society, 1986 , vol. 108, p. 6343
