2-羟基-4,6-二甲氧基苯乙酮合成路线 (共 113 条)
参考文献
Journal of the Chemical Society, , p. 91,93
参考文献
Proceedings - Indian Academy of Sciences, Section A, , vol. 23, p. 262,266
反应条件
und Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Yakugaku Zasshi, , p. 111
Chem. Zentralbl., , vol. 99, # I p. 333
反应条件
Kochen des Reaktionsprodukts mit Wasser;
参考文献
Journal of the Chemical Society, , p. 1255,1264
反应条件
potassium hydroxide in methanol T=20°C; Claisen condensation; 24 h;
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
反应条件
1.1: sodium peroxodisulphate; sodium hydroxide / water 2.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 3 h / -78 - -10 °C / |Inert atmosphere 2.2: -78 - 20 °C / |Inert atmosphere 2.3: |Cooling with ice 3.1: acetic acid; sulfuric acid / 3.5 h / 95 °C 4.1: lithium hydroxide hydrate / tetrahydrofuran; methanol / 2 h / 20 °C 5.1: magnesium bromide / acetonitrile / 3 h View Scheme
参考文献
Twincore Zentrum für Experimentelle und Klinische Infektionsforschung GmbH; CNRS Centre National de la Recherche Scientifique; Université de Strasbourg; Pietschmann, Thomas; Haid, Sibylle; Gentzsch, Juliane; Grethe, Christina; Davioud-Charvet, Elisabeth; Lanfranchi, Don Antoine; Elhabiri, Mourad; Benlloch-Martin, Xavier
Patent: EP2641904 A1, 2013 ;
反应条件
potassium hydroxide in methanol T=20°C; Claisen condensation; 24 h;
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
反应条件
in methanol; ethanol; water
参考文献
Hoffmann-La Roche Inc.
Patent: US4605674 A1, 1986 ;
反应条件
aluminium trichloride in chlorobenzene 1 h; Heating;
参考文献
Jain, A. C.; Gupta, S. M.; Bambah, Pawan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 393 - 397
反应条件
lt;Fe(DMF)3Cl2gt;lt;FeCl4gt; in methanol; water
参考文献
Parthasarathy,M.R. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15B, p. 942 - 944