乙基(甲基)-2-乙氧基-四氢-3-糠酸酯合成路线 （共 11 条）
反应条件
1: sulfuric acid / 125 °C 2: aqueous KOH-solution View Scheme
参考文献
Korte; Machleidt
Chemische Berichte, 1955 , vol. 88, p. 1676,1679
反应条件
1: sulfuric acid / 125 °C 2: aqueous KOH-solution 3: petroleum ether; thionyl chloride View Scheme
参考文献
Korte; Machleidt
Chemische Berichte, 1955 , vol. 88, p. 1676,1679
反应条件
disodium hydrogenphosphate; oxygen; dichloro bis(acetonitrile) palladium(II); copper(l) chloride in ethylene glycol dimethyl ether
参考文献
Hosokawa, Takahiro; Nakajima, Fumio; Iwasa, Shooji; Murahashi, Shun-Ichi
Chemistry Letters, 1990 , # 8 p. 1387 - 1390
反应条件
hydrogenchloride
1 h;
参考文献
AMAKEM NV; LEYSEN, Dirk; DEFERT, Olivier; KAVAL, Nadzeya; BLOM, Petra; BOLAND, Sandro
Patent: WO2011/107608 A1, 2011 ;
Location in patent: Page/Page column 80 ;
WO 2011/107608 A1
反应条件
pyridine; S-methylisothiourea sulfate
10 h; Heating;
参考文献
Madruga, Claudia da C.; Clerici, Edflia; Martins, Marcos A. P.; Zanatta, Nilo
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 735 - 738
反应条件
hydrogenchloride; sodium hydride
1.) ether, 20 h, 2.) 1 h; Yield given. Multistep reaction;
参考文献
Vader, Jan; Koopmans, Rimco; Groot, Aede De; Veldhuizen, Albertus van; Kerk, Sies van der
Tetrahedron, 1988 , vol. 44, # 9 p. 2663 - 2674
参考文献
Maynard-Faure; Gonser; Vaime; Bouchu
Tetrahedron Letters, 1998 , vol. 39, # 16 p. 2315 - 2318
反应条件
diethyl ether; ethanol; sodium
Erwaermen des Reaktionsprodukts mit Chlorwasserstoff enthaltendem Methanol;
参考文献
Korte; Machleidt
Chemische Berichte, 1955 , vol. 88, p. 1676,1679
参考文献
Korte; Machleidt
Chemische Berichte, 1955 , vol. 88, p. 136,142
参考文献
Korte; Machleidt
Chemische Berichte, 1955 , vol. 88, p. 1676,1679
