(1,3-二氢异苯并呋喃-5-基)甲醇合成路线 （共 6 条）
反应条件
(R)-(+)-N-benzyl-N-diphenylphosphino-2-methyl-2-propanesulfinamide; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen in 1,2-dichloro-ethane
T=20°C; 5 h; Inert atmosphere;
参考文献
Brun, Sandra; Parera, Magda; Pla-Quintana, Anna; Roglans, Anna; Leon, Thierry; Achard, Thierry; Sol, Jordi; Verdaguer, Xavier; Riera, Antoni
Tetrahedron, 2010 , vol. 66, # 46 p. 9032 - 9040
反应条件
hydrogenchloride; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; sodium chloride in diethyl ether
T=20°C; 24 h;
参考文献
Kinoshita, Hidenori; Shinokubo, Hiroshi; Oshima, Koichiro
Journal of the American Chemical Society, 2003 , vol. 125, # 26 p. 7784 - 7785
反应条件
methanol; sodium methylate
T=20°C; 1 h;
参考文献
BAYER CROPSCIENCE AG
Patent: WO2009/112275 A1, 2009 ;
Location in patent: Page/Page column 120-121 ;
反应条件
sodium tetrahydroborate; silica gel
T=40 - 45°C; 1 h;
参考文献
Liu, Wan-Yi; Xu, Qi-Hai; Ma, Yong-Xiang
Organic Preparations and Procedures International, 2000 , vol. 32, # 6 p. 596 - 600
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in acetone
T=60°C;
参考文献
Mallagaray, Alvaro; Medina, Sandra; Dominguez, Gema; Perez-Castells, Javier
Synlett, 2010 , # 14 art. no. G13410ST, p. 2114 - 2118
反应条件
ammonium chloride; magnesium
T=20°C; 3 h; Irradiation;
参考文献
Li, Ji-Tai; Bian, Yan-Jiang; Zang, Hong-Jun; Li, Tong-Shuang
Synthetic Communications, 2002 , vol. 32, # 4 p. 547 - 551
