(4-溴丁氧基)(叔丁基)二甲基硅烷合成路线 （共 5 条）
反应条件
1H-imidazole; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0°C; Substitution;
参考文献
Fuerstner, Alois; Mlynarski, Jacek; Albert, Martin
Journal of the American Chemical Society, 2002 , vol. 124, # 35 p. 10274 - 10275
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C;
参考文献
Fuerstner, Alois; Albert, Martin; Mlynarski, Jacek; Matheu, Maribel; DeClercq, Erik
Journal of the American Chemical Society, 2003 , vol. 125, # 43 p. 13132 - 13142
反应条件
tetrabutylammomium bromide; chlorodimethyl(phenylthio)chloride methanaminium in dichloromethane
T=20°C; Bromination;
参考文献
Gomez; Gellibert; Wagner; Mioskowski
Tetrahedron Letters, 2000 , vol. 41, # 32 p. 6049 - 6052
反应条件
lithium bromide in tetrahydrofuran
Heating;
参考文献
Nakashima, Katsuyuki; Okamoto, Sanae; Sono, Masakazu; Tori, Motoo
Molecules, 2004 , vol. 9, # 7 p. 541 - 549
反应条件
1: 70 percent / Et3N; DMAP / CH2Cl2 / 15 h / 20 °C
2: 23 percent / CBr4; Ph3P / CH2Cl2 / 0.08 h / 20 °C
View Scheme
参考文献
Yamada, Koji; Onaka, Hiroyuki; Tanaka, Masakazu; Inagaki, Masanori; Higuchi, Ryuichi
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 10 p. 1333 - 1334
