Hurd; Fancher
Journal of the American Chemical Society, 1947 , vol. 69, p. 716
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Hall; Turner
Journal of the Chemical Society, 1945 , p. 694,697
1: Cs2CO3 / dimethylformamide / 1.5 h
2: Et3N / CH2Cl2 / -78 - 20 °C
3: Cs2CO3; rac-2,2'-bis(diphenylphosphino)-1,1'-binaphthalene / Pd(OAc)2 / toluene / 16 h / 120 °C
4: barium hydroxide octahydrate / methanol / 90 °C
5: POCl3 / 2 h / 120 °C
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参考文献
Anderson, Marc O.; Sherrill, John; Madrid, Peter B.; Liou, Ally P.; Weisman, Jennifer L.; DeRisi, Joseph L.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 2 p. 334 - 343
1: Et3N / CH2Cl2 / -78 - 20 °C
2: Cs2CO3; rac-2,2'-bis(diphenylphosphino)-1,1'-binaphthalene / Pd(OAc)2 / toluene / 16 h / 120 °C
3: barium hydroxide octahydrate / methanol / 90 °C
4: POCl3 / 2 h / 120 °C
View Scheme
参考文献
Anderson, Marc O.; Sherrill, John; Madrid, Peter B.; Liou, Ally P.; Weisman, Jennifer L.; DeRisi, Joseph L.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 2 p. 334 - 343
1: Cs2CO3; rac-2,2'-bis(diphenylphosphino)-1,1'-binaphthalene / Pd(OAc)2 / toluene / 16 h / 120 °C
2: barium hydroxide octahydrate / methanol / 90 °C
3: POCl3 / 2 h / 120 °C
View Scheme
参考文献
Anderson, Marc O.; Sherrill, John; Madrid, Peter B.; Liou, Ally P.; Weisman, Jennifer L.; DeRisi, Joseph L.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 2 p. 334 - 343
1: barium hydroxide octahydrate / methanol / 90 °C
2: POCl3 / 2 h / 120 °C
View Scheme
参考文献
Anderson, Marc O.; Sherrill, John; Madrid, Peter B.; Liou, Ally P.; Weisman, Jennifer L.; DeRisi, Joseph L.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 2 p. 334 - 343
