2-(三甲基硅)苯基三氟甲烷磺酸盐合成路线 (共 525 条)
反应条件
copper(l) iodide; triphenylphosphine; cesium fluoride in acetonitrile
1 h; Inert atmosphereHeating;
参考文献
Xie, Chunsong; Zhang, Yuhong; Yang, Yuzhu
Chemical Communications, 2008 , # 39 p. 4810 - 4812
反应条件
copper(l) iodide; potassium carbonate; cesium fluoride; tri-cyclo-hexyl-phosphine in dichloromethane; acetonitrile
T=50°C; 5 h; Inert atmosphere;
参考文献
Bhuvaneswari, Sivakolundu; Jeganmohan, Masilamani; Cheng, Chien-Hong
Chemical Communications, 2008 , # 40 p. 5013 - 5015
反应条件
cesium fluoride in tetrahydrofuran
T=65°C; 24 h;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
cesium fluoride in acetonitrile
T=20°C; 16 h; Inert atmosphere;
参考文献
Dhokale, Ranjeet A.; Mhaske, Santosh B.
Organic Letters, 2013 , vol. 15, # 9 p. 2218 - 2221
反应条件
Ph2P(OMe); trifluoroacetic acid in tetrahydrofuran
T=0°C; 1 h;
参考文献
Yoshida, Suguru; Hosoya, Takamitsu
Chemistry Letters, 2013 , vol. 42, # 6 p. 583 - 585