2,4,6-三硝基氯苯合成路线 (共 249 条)
反应条件
ethanol; calcium carbonate
参考文献
Giua; de Franciscis
Ann.Chim.applic., vol. 15, p. 143
Chem. Zentralbl., 1926 , vol. 97, # I p. 225
参考文献
Giua; de Franciscis
Ann.Chim.applic., vol. 15, p. 139,143
Chem. Zentralbl., 1926 , vol. 97, # I p. 255
反应条件
1: 4-nitro-1H-imidazole With potassium hydroxide in N,N-dimethyl-formamide T=20°C; 1 h; 2: 2,4,6-trinitro-chlorobenzene With copper(l) iodide; tetrabutylammomium bromide in N,N-dimethyl-formamide T=20°C;
参考文献
Hou, Kehui; Liu, Zuliang
Chinese Journal of Chemistry, 2013 , vol. 31, # 2 p. 243 - 246
反应条件
(Ph3P)2Pd(Ph)(I) in 1,2-dichloro-ethane T=120 - 130°C; 1.5 h;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
反应条件
copper T=195 - 200°C;
参考文献
Gull; Turner
Journal of the Chemical Society, 1929 , p. 498
反应条件
sodium hydrogencarbonate in ethanol 0.166667 h; Ambient temperature;
参考文献
Atkins, Ronald L.; Nielsen, Arnold T.; Bergens, Cynthia; Wilson, William S.
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 503 - 507
反应条件
in water T=25°C; Rate constant;
参考文献
Stanciuc, Gabriela; Caproiu, M. Teodor; Caragheorgheopol, Agneta; Caldararu, Horia; Balaban, Alexandru T.; Walter, Robert I.
Journal of Magnetic Resonance (1969-1992), 1987 , vol. 75, # 1 p. 63 - 72
反应条件
potassium hydroxide in ethanol
参考文献
Stanciuc, Gabriela; Caproiu, M. Teodor; Caragheorgheopol, Agneta; Caldararu, Horia; Balaban, Alexandru T.; Walter, Robert I.
Journal of Magnetic Resonance (1969-1992), 1987 , vol. 75, # 1 p. 63 - 72
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Eli Lilly and Co.
Patent: FR2325325DE2642148 , 19771977 ;
Chem.Abstr., 1977 , vol. 87, # 52925
参考文献
Chapman; Fidler
Journal of the Chemical Society, 1936 , p. 448,451