bromine in benzene byproducts: MgBr2, MgBrCl; addition of C6F5MgBr (solution in ether) to a suspension of PbCl2 in benzene at 0°C under stirring; addition of Br2 in CH2Cl2 after 1 hour at 20°C;; evaporation and extraction with hexane;;
参考文献
Hills, K.; Henry, M. C.
Journal of Organometallic Chemistry, 1967 , vol. 9, p. 180 - 182
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Gmelin Handbook: F: PerFHalOrg.4, 4.4.1, page 190 - 191
Massey, A. G.; Park, A. J.
Journal of Organometallic Chemistry, 1964 , vol. 2, p. 461 - 465
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Gmelin Handbook: F: PerFHalOrg.4, 3.1.4.1.1, page 122 - 122
in diethyl ether reaction at 25°C, stirring for 12 hours;;
参考文献
Fenton, D. E.; Massey, A. G.; Urch, D. S.
Journal of Organometallic Chemistry, 1966 , vol. 6, p. 352 - 358
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Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169
in diethyl ether addition of SnCl4 (in n hexane) to C6F5MgBr in ether, evaporation of the ether after 3 hours and heating in butyl ether at 145°C, 3 hours;;
Tamborski, C.; Soloski, E. J.; Dec, S. M.
Journal of Organometallic Chemistry, 1965 , vol. 4, p. 446 - 454
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Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169
