2-甲基-2-苯基-1,3-二恶烷合成路线 （共 10 条）
反应条件
hydrogenchloride T=25°C; Rate constant;
参考文献
McClelland, Robert A.; Watada, Brian; Lew, Calvin S. Q.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 10 p. 1723 - 1728
反应条件
tungsten hexachloride; orthoformic acid triethyl ester in dichloromethane
0.916667 h; Ambient temperature;
参考文献
Firouzabadi; Iranpoor; Karimi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2255 - 2263
反应条件
iodine in dichloromethane
T=20°C; 66 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
N-halosuccinimide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
silver tetrafluoroborate; PPh3 gold(I) chloro complex in toluene
T=100°C; 4 h;
参考文献
Santos, Laura L.; Ruiz, Violeta R.; Sabater, Maria J.; Corma, Avelino
Tetrahedron, 2008 , vol. 64, # 34 p. 7902 - 7909
反应条件
1: water / acetonitrile-D3 / 0.33 h / UV-irradiation
2: tetra-n-butylammonium tribromide; trimethyl orthoformate / acetonitrile / 20 °C
View Scheme
参考文献
Thevenet, Damien; Neier, Reinhard
Helvetica Chimica Acta, 2011 , vol. 94, # 2 p. 331 - 346
反应条件
1: water / acetonitrile-D3 / 0.33 h / UV-irradiation
2: tetra-n-butylammonium tribromide; trimethyl orthoformate / acetonitrile / 20 °C
View Scheme
参考文献
Thevenet, Damien; Neier, Reinhard
Helvetica Chimica Acta, 2011 , vol. 94, # 2 p. 331 - 346
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
H3[PW12O40] in Petroleum ether
2 h; Heating;
参考文献
Firouzabadi; Iranpoor; Amani
Synthesis, 2002 , # 1 p. 59 - 62
