4-(三甲基甲硅烷基)苯甲醚合成路线 (共 34 条)
反应条件
sodium in toluene T=20°C; Wurtz-Fittig reaction; Product distribution; Further Variations:ReagentsReaction partnersSolvents;
参考文献
Journal of Organic Chemistry, , vol. 72, # 21 p. 8107 - 8110
反应条件
bis(cyclopentadienyl)titanium dichloride; manganese in tetrahydrofuran Michael-type addition; 5 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 8 p. 4171 - 4176
反应条件
1: ozone / dichloromethane / -78 °C 2: manganese; bis(cyclopentadienyl)titanium dichloride / tetrahydrofuran / 0.5 h / Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 77, # 8 p. 4171 - 4176
反应条件
sodium in toluene T=20°C; Wurtz-Fittig reaction; 23 h; Product distribution; Further Variations:Solvents;
参考文献
Journal of Organic Chemistry, , vol. 72, # 21 p. 8107 - 8110
反应条件
in benzene-d6 20 h; UV-irradiationInert atmosphere;
参考文献
Organometallics, , vol. 29, # 4 p. 1041 - 1044
反应条件
lead(IV) acetate; boron trifluoride diethyl etherate Ambient temperature;
参考文献
Meio, Giuseppe V. De; Pinhey, John T.
Journal of the Chemical Society, Chemical Communications, 1990 , # 15 p. 1065 - 1066
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De Meio; Morgan; Pinhey
Tetrahedron, 1993 , vol. 49, # 36 p. 8129 - 8138
反应条件
cesium fluoroxysulphate; boron trifluoride diethyl etherate in acetonitrile Ambient temperature; Title compound not separated from byproducts;
参考文献
Diorazio; Widdowson; Clough
Tetrahedron, 1992 , vol. 48, # 37 p. 8073 - 8088
反应条件
Stirring of silane with a slurry of Pb(OAc)4 in excess of BF3*Et2O overnight at room temp.; GC anal.;
参考文献
Meio, Giuseppe V. De; Pinhey, John T.
Journal of the Chemical Society, Chemical Communications, 1990 , # 15 p. 1065 - 1066
反应条件
silver tetrafluoroborate; iodine cloride in methanol T=0°C; 0.0833333 h;
参考文献
Jacob; Chen; Stec
Synthesis, 1993 , # 6 p. 611 - 614
反应条件
HCl in acetic acid byproducts: methoxybenzene; introduction of gaseous HCl into a boiling soln. of (CH3)3SiC6H4OCH3 in glacial acetic acid;;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4528 - 4531
Journal of the American Chemical Society, , vol. 71, p. 2066 - 2069
Journal of the American Chemical Society, , vol. 72, p. 2629 - 2632
Si: MVol.C, 21, page 66 - 68